HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrabutylammonium Fluoride → HCID 18790896, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrabutylammonium Fluoride | HCID 2724141 | — |
| Reactant | HCID 18790897 | HCID 18790897 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 18790896 | HCID 18790896 | — |
Reaction Steps
8-(tert-butyldimethylsilyloxy)-3-butyloct-1-ene (4.0 g, 13.4 mmol) was added to a solution of tetrabutylammonium fluoride (1 M, 14 ml) in THF, and the mixture was stirred at ambient temperature for 24 h. Standard work-up followed by PMPLC yielded 2.05 g (83%) of 6-butyl-7-en-1-ol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06054141 |
| Source dataset | uspto-grants-2000_04 |
| ORD ID | ord-e0dbc86556564279a5ad31c3be09c44a |
| Source note | uspto-grants-2000_04 |