HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylhydrazine → HCID 67650044, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylhydrazine | HCID 6061 | — |
| Reactant | 4-Chloro-2-fluorobenzaldehyde | HCID 2724908 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 67650044 | HCID 67650044 | 94% |
Reaction Steps
5.5 g (0.12 mol) of methylhydrazine were added to a solution of 19 g (0.12 mol) of 4-chloro-2-fluorobenzaldehyde in 120 ml of ethanol. After 1 hour, the mixture was concentrated, and the residue was subsequently treated with ethyl acetate. The organic phase was washed with water, dried over magnesium sulfate and finally concentrated. Yield: 94%
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06054412 |
| Source dataset | uspto-grants-2000_04 |
| ORD ID | ord-b1535c9a0e3d493bbd5a5071f86d6458 |
| Source note | uspto-grants-2000_04 |