HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18791148, compound → HCID 18791127, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18791148 | HCID 18791148 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 18791127 | HCID 18791127 | — |
Reaction Steps
A solution of methyl N-formyl-α-(3,3-diethoxycarbonylcyclobutylidene)glycinate (0.46 g, 1.47 mmol) in ethanol (40 ml) was hydrogenated over 10% palladium-carbon (100 mg) at 65 psi for 24 hours. The reaction mixture was filtered through a pad of celite and evaporated to give a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06054448 |
| Source dataset | uspto-grants-2000_04 |
| ORD ID | ord-51bc421d419f40ceaa2828a45a2e222c |
| Source note | uspto-grants-2000_04 |