HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pentanoyl chloride, 4-methyl- → 2-(4-Methyl-1-oxopentyl)furan
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pentanoyl chloride, 4-methyl- | HCID 170008 | — |
| Reactant | 2-(Tributylstannyl)furan | HCID 4393688 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 2-(4-Methyl-1-oxopentyl)furan | HCID 95287 | — |
Reaction Steps
A solution of 2-tributylstannylfuran (1 mmol), 4-methylvaleroyl chloride (1.1 mmol), and PdCl2 (PPh3)2 (0.05 mmol) in THF was stirred at 25° C. for 24 h. Extraction and chromatography gave 2-(4-methylvaleryl)furan.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06054587 |
| Source dataset | uspto-grants-2000_04 |
| ORD ID | ord-adb24a006c4146be9f91db17b35a99ab |
| Source note | uspto-grants-2000_04 |