HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-[5-(3,5-Dimethyl-phenylsulfanyl)-4-isopropyl-2-methyl-imidazol-1-ylmethoxy]-ethanol → HCID 17776718, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-[5-(3,5-Dimethyl-phenylsulfanyl)-4-isopropyl-2-methyl-imidazol-1-ylmethoxy]-ethanol | HCID 478180 | — |
| Reactant | 1-methoxycycloheptene | HCID 11029851 | — |
| Product | HCID 17776718 | HCID 17776718 | 77% |
Reaction Steps
The compound 1 (401 mg, 1.20 mmol) was converted to the enol ether with 1-methoxy-1-cycloheptene (1.51 g, 12.0 mmol) in the same manner as the example 7 to give the compound 7 (372 mg, 77%) as oil. Rf 0.75 (Al2O3 60-type E, 2:1 hexane -EtOAc).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06054591 |
| Source dataset | uspto-grants-2000_04 |
| ORD ID | ord-75f81a0568c84c17b2e6504481baf651 |
| Source note | uspto-grants-2000_04 |