Sodium Chloride → HCID 131724579, compound

HRID 1005619Notes

Reaction equation

HRID 1005619 reaction equation
[CH3:1][S:2]([Cl:5])(=[O:4])=[O:3].[Cl-:6].[Cl-].[Cl-].[Al+3:9].[Cl-].[Na+:11]>>[CH3:1][S:2]([Cl:5])(=[O:4])=[O:3].[Cl-:6].[Cl-:5].[Cl-:5].[Al+3:9].[Cl-:5].[Na+:11]

Participants

4

Reactant 3

HCID 5234Sodium ChlorideHCID 31297Methanesulfonyl chlorideHCID 6451240Aluminum(III) Chloride

Product 1

HCID 131724579HCID 131724579, compound

Conditions

Temperature
60 °C

Procedure

A room temperature ionic solution was prepared by initially adding methanesulfonyl chloride (458.4 g, 4.0 mole) to a flask same as described above. Aluminum trichloride (746.8 g, 5.6 mole) was added over a three hour period, keeping the temperature below 50° C. The solution was then heated to 60° C. and sodium chloride (93.6 g, 1.6 mole) was added over 0.5 hour, keeping the temperature below 70° C. The reaction was cooled to room temperature to give a clear green solution.

Workup

  1. customthe temperature below 50° C
  2. customthe temperature below 70° C
  3. temperatureThe reaction was cooled to room temperature
  4. customto give a clear green solution

Sources & evidence

ORD record
ord-470d9eb2968543dcaa4c16abaeb1c01c
Source dataset
uspto-grants-2004_09
Patent number
US06787019B2

Reaction notes

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