Sodium Chloride → HCID 131724579, compound

Participants

Reaction Conditions

Reaction Steps

A room temperature ionic solution was prepared by initially adding methanesulfonyl chloride (458.4 g, 4.0 mole) to a flask same as described above. Aluminum trichloride (746.8 g, 5.6 mole) was added over a three hour period, keeping the temperature below 50° C. The solution was then heated to 60° C. and sodium chloride (93.6 g, 1.6 mole) was added over 0.5 hour, keeping the temperature below 70° C. The reaction was cooled to room temperature to give a clear green solution.

Provenance & Evidence