Hydrochloric Acid → HCID 22674054, compound

Participants

Reaction Steps

In ethanol (5 ml) was dissolved 1.173 g of N-Boc-1-methyl-2-(3-ethoxycarbonylaminophenyl)ethylamine (crude), and hydrochloric acid (5 ml) was added thereto, followed by stirring at room temperature for 1.5 hours. Then, hydrochloric acid (2.5 ml) was further added thereto, followed by stirring at room temperature for 2 hours. The solvent was evaporated, to give the title compound (1.148 g, crude) as a yellow oil. The obtained compound was subjected to the subsequent reaction as intact without further purification.

Provenance & Evidence