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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1005711Generated: November 2, 2026

Hydrochloric Acid → HCID 22674466, compound

https://huagongshe.com/reaction/1005711

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 22674383HCID 22674383—
SolventMethanolHCID 887—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 22674466HCID 2267446677%

Reaction Steps

A solution of 2-(2-butoxycarbonylaminoethylamino)thieno[3,2-d]pyrimidin-4-yl 2-thienylmethanone (58 mg, 0.14 mmol) in MeOH (5 mL) was treated with 4-M HCl in dioxane (0.5 mL), stirred at room temperature for 16 h and the resulting solid filtered and washed with ether to give the title compound (41 mg, 77%) as a white crystalline solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06787541B1
Source datasetuspto-grants-2004_09
ORD IDord-6e75937168a246419193d4998cb1c85a
Source noteuspto-grants-2004_09