HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl isocyanate → HCID 22674417, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl isocyanate | HCID 15123 | — |
| Reactant | HCID 22674428 | HCID 22674428 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 22674417 | HCID 22674417 | 68% |
Reaction Steps
A mixture of 2-hydrazinothieno[3,2-d]pyrimidin-4-yl 2-thienylmethanone (100 mg, 0.36 mmol) and THF (5 mL) was treated with allyl isocyanate (32 μl, 0.36 mmol), stirred at room temperature for 1 h and filtered to give the title compound (88 mg, 68%) as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06787541B1 |
| Source dataset | uspto-grants-2004_09 |
| ORD ID | ord-920c89a828734e7990aed4e5e0eca1f1 |
| Source note | uspto-grants-2004_09 |