HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl cyclohexanecarboxylate → Methyl 1-(iodomethyl)cyclohexanecarboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl cyclohexanecarboxylate | HCID 20748 | — |
| Reactant | 4-Iodomethyl-tetrahydro-pyran-4-carboxylic acid methyl ester | HCID 22719788 | — |
| Product | Methyl 1-(iodomethyl)cyclohexanecarboxylate | HCID 58947958 | 100% |
Reaction Steps
Prepared according to the method for the preparation of 4-iodomethyltetrahydropyran-4-carboxylic acid methyl ester, from cyclohexane-carboxylic acid methyl ester (10 ml), to give the title compound as a brown gum (20 g, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06787536B2 |
| Source dataset | uspto-grants-2004_09 |
| ORD ID | ord-2efadd1307e64ed6a9b3aebd237fa48d |
| Source note | uspto-grants-2004_09 |