HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(R)-benzyl-3-(2-(R)-chlorosulfonylmethyl-3 methylbutyryl)oxazolidin-2-one → 1-Chlorosulfonylmethylcyclohexanecarboxylic acid methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(R)-benzyl-3-(2-(R)-chlorosulfonylmethyl-3 methylbutyryl)oxazolidin-2-one | HCID 22888284 | — |
| Reactant | 1-Acetylsulfanyl-methylcyclohexanecarboxylic acid methyl ester | HCID 86590245 | — |
| Product | 1-Chlorosulfonylmethylcyclohexanecarboxylic acid methyl ester | HCID 58947956 | 96% |
Reaction Steps
Prepared according to the method for the preparation of 4-(R)-benzyl-3-(2-(R)-chlorosulfonylmethyl-3-methyl butyryl)oxazolidin-2-one, from 1-acetylsulfanyl-methylcyclohexanecarboxylic acid methyl ester (20 g), to provide the title compound as a red oil (14 g, 96%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06787536B2 |
| Source dataset | uspto-grants-2004_09 |
| ORD ID | ord-13153a13a3aa4509aa6323659d94fb9d |
| Source note | uspto-grants-2004_09 |