HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 69920491, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 69920246 | HCID 69920246 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 69920491 | HCID 69920491 | — |
Reaction Steps
To a solution of 4-[2-(N-isopropyl-phenylsulfonylamino)-5-trifluoromethylphenoxymethyl]cinnamic acid (425 mg; prepared in Example 18(40).) in MeOH (5 ml), 2N NaOH (0.41 ml) was added. The mixture was stirred at room temperature. The mixture was distilled off azeotropically with benzene three times to give the title compound (430 mg) having the following physical data.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06790866B2 |
| Source dataset | uspto-grants-2004_09 |
| ORD ID | ord-79d65e22f02940b788fc3d43885b4faf |
| Source note | uspto-grants-2004_09 |