HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69431580, compound → HCID 69429829, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69431580 | HCID 69431580 | — |
| Solvent | Tetrahydrofuran ethanol | HCID 21873804 | — |
| Product | HCID 69429829 | HCID 69429829 | — |
Reaction Steps
Hydrolysis in EtOH/THF (see General method for hydrolysis of an ester): (R)- or (S)-2-[(2S,4R)-1-methanesulfonyl-4-tritylsulfanyl-pyrrolidin-2-ylmethoxy]-4-methyl-pentanoic acid methyl ester gave (R)- or (S)-2-[(2S,4R)-1-methanesulfonyl-4-tritylsulfanyl-pyrrolidin-2-ylmethoxy]-4-methyl-pentanoic acid, MS: 568 (MH+); and (S)- or (R)-2-[(2S,4R)-1-methanesulfonyl-4-tritylsulfanyl-pyrrolidin-2-ylmethoxy]-4-methyl-pentanoic acid methyl ester gave (R)- or (S)-2-[(2S,4R)-1-Methanesulfonyl-4-tritylsulfanyl-pyrrolidin-2-ylmethoxy]-4-methyl-pentanoic acid, MS: 568 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06790860B2 |
| Source dataset | uspto-grants-2004_09 |
| ORD ID | ord-7622812425634fa9a986af724e29cc87 |
| Source note | uspto-grants-2004_09 |