HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitric Acid → HCID 86588304, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | Cefazolin | HCID 33255 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 86588304 | HCID 86588304 | 60% |
Reaction Steps
The compound is prepared by adding to a Cefazolin solution (1.5 g, 3.3 mmoles) in methanol (50 ml) a 65% nitric acid solution (0.250 ml) in acetonitrile (5 ml) and following then the procedure reported in Example 5. Cefazolin nitrate as amorphous solid is obtained. Yield 60%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06794372B2 |
| Source dataset | uspto-grants-2004_09 |
| ORD ID | ord-955def51e9aa40919ef80b0db6be4116 |
| Source note | uspto-grants-2004_09 |