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HRID1007178

反应详情

EQUATION

反应方程式

HRID 1007178 的结构方程式

REACTANTS

反应物

2
结构：Nc1ccc(Cl)cc1[N+](=O)[O-]
HCID6979

4-Chloro-2-nitroaniline

C6H5ClN2O2

结构：O=C(Cl)c1ccc(Cl)nc1
HCID2782165

6-Chloropyridine-3-carbonyl chloride

C6H3Cl2NO

PRODUCTS

生成物

1
结构：O=C(Nc1ccc(Cl)cc1[N+](=O)[O-])c1ccc(Cl)nc1
HCID9836371

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 6-chloronicotinoyl chloride and 4-chloro-2-nitroaniline and was obtained as a yellow solid as described in Example 1. 1H NMR (DMSO-d6): 11.31 (s, 1H), 9.02 (d, J=2.4, 1H), 8.96 (d, J=9.3, 1H), 8.31 (d, J=2.4, 1H), 8.24-8.20 (m, 1H), 7.73-7.69 (m, 1H), 7.54 (d, J=8.4, 1H).

WORKUP

后处理

  1. customwas obtained as a yellow solid