HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloro-2-nitroaniline → 6-Chloro-N-(4-chloro-2-nitrophenyl)-3-pyridinecarboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloro-2-nitroaniline | HCID 6979 | — |
| Reactant | 6-Chloronicotinoyl Chloride | HCID 2782165 | — |
| Product | 6-Chloro-N-(4-chloro-2-nitrophenyl)-3-pyridinecarboxamide | HCID 9836371 | — |
Reaction Steps
The title compound was prepared from 6-chloronicotinoyl chloride and 4-chloro-2-nitroaniline and was obtained as a yellow solid as described in Example 1. 1H NMR (DMSO-d6): 11.31 (s, 1H), 9.02 (d, J=2.4, 1H), 8.96 (d, J=9.3, 1H), 8.31 (d, J=2.4, 1H), 8.24-8.20 (m, 1H), 7.73-7.69 (m, 1H), 7.54 (d, J=8.4, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06794397B2 |
| Source dataset | uspto-grants-2004_09 |
| ORD ID | ord-8b1ecd6f631747bea5b93356b137fea8 |
| Source note | uspto-grants-2004_09 |