HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Ethoxy-2-nitroaniline → 2,5-Dimethyl-N-(4-ethoxy-2-nitrophenyl)-3-furancarboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Ethoxy-2-nitroaniline | HCID 69229 | — |
| Reactant | 2,5-Dimethyl-3-furoic acid | HCID 69465 | — |
| Product | 2,5-Dimethyl-N-(4-ethoxy-2-nitrophenyl)-3-furancarboxamide | HCID 22668918 | — |
Reaction Steps
The title compound was prepared from 2,5-dimethyl-3-furoic acid and 4-ethoxy-2-nitroaniline as an orange solid as described in Example 15. 1H NMR (CDCl3): 10.59 (s, 1H), 8.83 (d, J=9.0, 1H), 7.70 (d, J=3.0, 1H), 7.27-7.25 (m, 1H), 6.24 (s, 1H), 4.08 (q, J=6.9, 2H), 2.62 (s, 3H), 2.30 (s, 3H), 1.45 (t, J=6.9, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06794397B2 |
| Source dataset | uspto-grants-2004_09 |
| ORD ID | ord-457bd0b0a03f4b0882214653708f43bf |
| Source note | uspto-grants-2004_09 |