HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-5-bromo-3-nitropyridine → 6-Chloro-N-(5-bromo-3-nitro-2-pyridyl)-3-pyridinecarboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-5-bromo-3-nitropyridine | HCID 138878 | — |
| Reactant | 6-Chloronicotinoyl Chloride | HCID 2782165 | — |
| Product | 6-Chloro-N-(5-bromo-3-nitro-2-pyridyl)-3-pyridinecarboxamide | HCID 22668934 | — |
Reaction Steps
The title compound was prepared from 6-chloronicotinoyl chloride and 2-amino-5-bromo-3-nitropyridine as a light yellow solid as described in Example 1. 1H NMR (CDCl3): 10.56 (s, 1H), 9.00 (d, J=2.7, 1H), 8.82 (d, J=2.1, 1H), 8.69 (d, J=2.1, 1H), 8.27-8.23 (m, 1H), 7.53 (d, J=8.1, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06794397B2 |
| Source dataset | uspto-grants-2004_09 |
| ORD ID | ord-9516a97397d44db1ae37d2826ef21a5c |
| Source note | uspto-grants-2004_09 |