HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Nitro-2,4-xylidine → HCID 9857686, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Nitro-2,4-xylidine | HCID 74219 | — |
| Reactant | 6-Chloronicotinoyl Chloride | HCID 2782165 | — |
| Product | HCID 9857686 | HCID 9857686 | — |
Reaction Steps
The title compound was prepared from 6-chloronicotinoyl chloride and 2-nitro-4,6-dimethylaniline as a light yellow solid as described in Example 1. 1H NMR (CDCl3): 9.09 (s, 1H), 8.97 (d, J=2.4, 1H), 8.22-8.18 (m, 1H), 7.60 (d, J=1.2, 1H), 7.50 (d, J=8.1, 1H), 7.42 (s, 1H), 2.43 (s, 3H), 2.35 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06794397B2 |
| Source dataset | uspto-grants-2004_09 |
| ORD ID | ord-71d6dbfa9bdb4feb8c1a5aedcf183925 |
| Source note | uspto-grants-2004_09 |