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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1007222Generated: October 25, 2026

6-Chloronicotinoyl Chloride → 6-Chloro-N-(4,5-dimethoxy-2-nitrophenyl)-3-pyridinecarboxamide

https://huagongshe.com/reaction/1007222

Reaction equation

Participants

RoleNameHCIDCharge
Reactant6-Chloronicotinoyl ChlorideHCID 2782165—
Reactant4,5-Dimethoxy-2-nitroanilineHCID 4653152—
Product6-Chloro-N-(4,5-dimethoxy-2-nitrophenyl)-3-pyridinecarboxamideHCID 10290894—

Reaction Steps

The title compound was prepared from 6-chloronicotinoyl chloride and 4,5-dimethoxy-2-nitroaniline as a yellow solid as described in Example 1. 1H NMR (CDCl3): 11.84 (s, 1H), 9.04 (d, J=1.8, 1H), 8.66 (s, 1H), 8.25-8.21 (m, 1H), 7.77 (s, 1H), 7.53 (d, J=8.7, 1H), 4.07 (s, 3H), 3.97 (s, 3H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06794397B2
Source datasetuspto-grants-2004_09
ORD IDord-0a3f719bd6324958999e9d5e5ee60f32
Source noteuspto-grants-2004_09