HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 178501209, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 178511566 | HCID 178511566 | — |
| Product | HCID 178501209 | HCID 178501209 | — |
Reaction Steps
A solution of 2.0 g of cis-4-aminocyclohexanecarboxylic acid in 20 mL of methanol was combined with 3.57 mL of thionyl chloride, and stirred for 3 hours. The reaction solution was concentrated, and the residue was washed with ethyl ether to obtain 2.64 g of the desirable compound as colorless crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06794389B2 |
| Source dataset | uspto-grants-2004_09 |
| ORD ID | ord-045e3cd6d56142f994399d3401151979 |
| Source note | uspto-grants-2004_09 |