HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86587751, compound → HCID 22669529, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86587751 | HCID 86587751 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 22669529 | HCID 22669529 | — |
Reaction Steps
Analogously to the procedure of Example 25, 0.2 g (0.38 mmol) of 3-oxopentene-4-Carboxylic acid derivative from Example 26 is hydrogenated overnight in methanol with palladium on active carbon under a hydrogen atmosphere. The crude product is chromatographed on silica gel using toluene/ethyl acetate (10:1) in the isocratic mode.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06794406B2 |
| Source dataset | uspto-grants-2004_09 |
| ORD ID | ord-f7784b8fa119432d8fb8fd268eb35508 |
| Source note | uspto-grants-2004_09 |