Hydrochloric Acid → HCID 22666516, compound

Participants

Reaction Steps

In 2.5 mL of ethyl acetate is dissolved 0.49 g of N-[2-(2-benzo[b]thiophen-7-ylethoxy)ethyl]-N,N-dimethylamine, to which is added 0.73 mL of 3.5 mol/L solution of dry hydrogen chloride in ethyl acetate. The resulting solution is stirred at ambient temperature for one hour. The deposited crystal is collected by filtration, washed with ethyl acetate and dried to obtain 0.44 g of N-[2-(2-benzo[b]thiophen-7-ylethoxy)ethyl]-N,N-dimethylamine hydrochloride.

Provenance & Evidence