HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 22666336, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 22666265 | HCID 22666265 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22666336 | HCID 22666336 | — |
Reaction Steps
In 3 mL of ethanol is dissolved 0.23 g of 2-(methyl{2-[2-(6-quinoxalinyl)ethoxy]ethyl}amino)-1-ethanol, to which is added 0.8 mL of 3.8 mol/L solution of dry hydrogen chloride in ethanol. The mixture is stirred at ambient temperature for one hour. By distilling off the solvent under reduced pressure, there is obtained 0.67 g of 2-(methyl{2-[2-(6-quinoxalinyl)-ethoxy]ethyl}amino)-1-ethanol trihydrochloride as an oily product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06797726B1 |
| Source dataset | uspto-grants-2004_09 |
| ORD ID | ord-793bf4a9f14546a5be720fd77669c16a |
| Source note | uspto-grants-2004_09 |