Hydrochloric Acid → HCID 22666489, compound

HRID 1007909Notes

Reaction equation

HRID 1007909 reaction equation
[CH3:1][O:2][C:3]1[C:11]([CH2:12][CH2:13][O:14][CH2:15][CH2:16][N:17]([CH3:21])[CH2:18][CH2:19][OH:20])=[CH:10][C:6]2[O:7][CH:8]=[CH:9][C:5]=2[CH:4]=1.[ClH:22]>O>[ClH:22].[CH3:1][O:2][C:3]1[C:11]([CH2:12][CH2:13][O:14][CH2:15][CH2:16][N:17]([CH3:21])[CH2:18][CH2:19][OH:20])=[CH:10][C:6]2[O:7][CH:8]=[CH:9][C:5]=2[CH:4]=1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 22666365HCID 22666365, compound

Product 1

HCID 22666489HCID 22666489, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

In a mixture of 0.21 mL of 6 mol/L hydrochloric acid and 1 mL of water is dissolved 0.37 g of 2-[[2-(2-(5-methoxybenzo[b]furan-6-yl)ethoxy]ethyl}-(methyl)amino]-1-ethanol. The resulting solution is frozen and water is distilled off therefrom under reduced pressure. Thus, 0.40 g of 2-[{2-[2-(5-methoxybenzo[b]furan-6-yl)ethoxy]-ethyl}(methyl)amino]-1-ethanol hydrochloride is obtained as an oily product.

Workup

  1. temperatureThe resulting solution is frozen
  2. distillationwater is distilled off

Sources & evidence

ORD record
ord-369c3521177e491f82fb7924952e1c14
Source dataset
uspto-grants-2004_09
Patent number
US06797726B1

Reaction notes

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