HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 22666474, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 22666263 | HCID 22666263 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 22666474 | HCID 22666474 | — |
Reaction Steps
In 10 mL of benzene is dissolved 0.73 g of 2-[2-(6-quinoxalinyl)ethoxy]-1-ethanol, to which is added 0.32 mL of thionyl chloride. The mixture is heated under reflux for 30 minutes. The solvent is distilled off and the deposited crystal is collected by filtration to obtain 0.37 g of 6-[2-(2-chloroethoxy)-ethyl]-quinoxaline hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06797726B1 |
| Source dataset | uspto-grants-2004_09 |
| ORD ID | ord-e0349c1878ee4dbe9093006211846655 |
| Source note | uspto-grants-2004_09 |