Dimethylsulphamoyl chloride → N'-{2-[2-(4-Amino-2,6,7-trimethyl-1H-imidazo[4,5-c]pyridin-1-yl)ethoxy)ethyl}-N,N-dimethylsulfamide

Participants

Role	Name	HCID	Charge
Reactant	Dimethylsulphamoyl chloride	HCID 83372	—
Reactant	1-[2-(2-aminoethoxy)ethyl]-2,6,7-trimethyl-1H-imidazo[4,5-c]pyridin-4-amine	HCID 21913053	—
Product	N'-{2-[2-(4-Amino-2,6,7-trimethyl-1H-imidazo[4,5-c]pyridin-1-yl)ethoxy)ethyl}-N,N-dimethylsulfamide	HCID 21913134	—

Reaction Steps

Using the method of Examples 34-50, dimethylsulfamoyl chloride was reacted with 1-[2-(2-aminoethoxy)ethyl]-2,6,7-trimethyl-1H-imidazo[4,5-c]pyridin-4-amine to provide the desired compound. The product was purified using Method A. The observed accurate mass was 371.1861.

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US06797718B2
Source dataset	uspto-grants-2004_09
ORD ID	ord-806dda5854fd42de9d43d59982d63deb
Source note	uspto-grants-2004_09