HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1008105Generated: October 25, 2026
Trichloroacetonitrile → 3-{4-[2,4-bis(trichloromethyl)-s-triazine-6-yl]phenyl thio}propionic Acid
https://huagongshe.com/reaction/1008105
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Trichloroacetonitrile | HCID 11011 | — |
| Reactant | Aluminum bromide | HCID 24409 | — |
| Reactant | 3-[(4-Cyanophenyl)sulfanyl]propanoic acid | HCID 22666602 | — |
| Product | 3-{4-[2,4-bis(trichloromethyl)-s-triazine-6-yl]phenyl thio}propionic Acid | HCID 60111243 | — |
Reaction Steps
The reaction mixture of 22 g of 3-(4-cyanophenyl thio)propionic acid, 150 g of trichloroacetonitrile, and 2 g of AlBr3 was heated to 60° C. in order to dissolve the initially undissolved starting materials, and was bubbled by dry HCl at room temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06797739B1 |
|---|
| Source dataset | uspto-grants-2004_09 |
|---|
| ORD ID | ord-55159e626f014794ad064a59718bac78 |
|---|
| Source note | uspto-grants-2004_09 |
|---|
