N-(6-formyl-1-isoquinolinyl)benzamide → N-(7-Formylisoquinolinyl)benzamide

Participants

Role	Name	HCID	Charge
Reactant	N-(6-formyl-1-isoquinolinyl)benzamide	HCID 22665740	—
Reactant	N-(7-bromo-1-isoquinolinyl)benzamide	HCID 22665843	—
Product	N-(7-Formylisoquinolinyl)benzamide	HCID 22665912	—

Reaction Steps

N-(7-Formylisoquinolinyl)benzamide was prepared from 37e using the procedure described for 1f but was not purified using column chromatography. The crude aldehyde was transformed into the title compound using the procedure described for 1g folowed by purification using column chromatography on silica gel (toluene/ethyl acetate: 2/1). M.p. 137.5-139.0° C.

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US06797710B2
Source dataset	uspto-grants-2004_09
ORD ID	ord-e1615c706a074bc99a7aa1cd7ba2a707
Source note	uspto-grants-2004_09