HuagongsheHuagongshe Chemistry Print Report · For research reference only
Urocanic Acid → HCID 178525356, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Urocanic Acid | HCID 736715 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178525356 | HCID 178525356 | — |
Reaction Steps
Urocanic acid (3-(1H-imidazol-4-yl)-acrylic acid) (138 mg, 1 mmol) was placed in a round-bottom flask and dist MeOH was added thereto until urocanic acid was completely dissolved. To this solution, 10% Pd/C (30 mg) was added, replaced with H2 and stirred. After five hours, the loss of raw materials was confirmed, filtered, and the filtrate was concentrated under a reduced pressure to give the objective product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07973027B2 |
| Source dataset | uspto-grants-2011_07 |
| ORD ID | ord-007396ff74da472dba05514217e4cb3d |
| Source note | uspto-grants-2011_07 |