Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-Aminoheptanoic acid | HCID 227939 | — |
| Product | HCID 23074222 | HCID 23074222 | — |
Reaction Steps
Thionyl chloride (2.19 g) (supplied from Wako Pure Chemical Industries) was added dropwise to a suspension of 2.18 g of 2-aminoheptanoic acid in 50 mL of methanol, and stirred at 60° C. overnight. Methanol and thionyl chloride were distilled off, and the residue was washed with 20 mL of ether, to yield 2.84 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07973030B2 |
|---|
| Source dataset | uspto-grants-2011_07 |
|---|
| ORD ID | ord-cbed6ce868b44b4cb3424282e166a3e6 |
|---|
| Source note | uspto-grants-2011_07 |
|---|
