HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → HCID 16657408, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 54684476 | HCID 54684476 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 16657408 | HCID 16657408 | — |
Reaction Steps
1-(2,4-dichloro-benzyl)-4-hydroxy-1H-pyridin-2-one synthesized in Example 14 was dissolved in DMF followed by adding NaH and benzyl bromide to obtain 4-benzyloxy-1-(2,4-dichloro-benzyl)-1H-pyridin-2-one and the titled compound in the ratio of 1:1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07973060B2 |
| Source dataset | uspto-grants-2011_07 |
| ORD ID | ord-78b978a5dc8244d18a2e2bd548a24f49 |
| Source note | uspto-grants-2011_07 |