Azobisisobutyronitrile → HCID 86619238, compound

Participants

Reaction Steps

Acrylic acid (4.2 g), 2,2,3,4,4,4-hexafluorobutyl methacrylate (14 g), t -butyl acrylate (14 g) and styrene (8.26 g) were mixed with azobisisobutyronitrile (AIBN) (4 g) as a polymerization initiator and propyleneglycol methyl ether acetate (PGMEA) (145 g) as a polymerization solvent. The resulting mixture was reacted at approximately 67° C. for approximately 12 hours, and precipitated in normal hexane and dehydrated to obtain an organic polymer compound with yield of approximately 82% (see FIG. 3).

Provenance & Evidence