HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl cyanoacetate → 3-Hydroxybenzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl cyanoacetate | HCID 7764 | — |
| Reactant | Cyclopropyl methyl ketone | HCID 13004 | — |
| Product | 3-Hydroxybenzaldehyde | HCID 101 | — |
| Product | Ammonium Acetate | HCID 517165 | — |
Reaction Steps
Analogously to Example 1a, 750 mg of product is obtained from 5 g of ammonium acetate, 875 μl of cyanoacetic acid ethyl ester, 815 μl of cyclopropylmethylketone and 1 g of 3-hydroxybenzaldehyde.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07977325B2 |
| Source dataset | uspto-grants-2011_07 |
| ORD ID | ord-45b050a4b7e6406f9586176aecc8ba06 |
| Source note | uspto-grants-2011_07 |