HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl isothiocyanate → HCID 57813664, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl isothiocyanate | HCID 68284 | — |
| Reactant | HCID 57813693 | HCID 57813693 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 57813664 | HCID 57813664 | 89% |
Reaction Steps
To the solution of 3-bromo-5-pyrazol-1-yl-phenylamine (0.18 g, 0.76 mmol) in anhydrous acetone (5.0 mL) was added benzoylisothiocyanate (0.14 g, 0.83 mmol) and the reaction mixture was stirred at room temperature for 30 min. Acetone was distilled off and the crude residue was washed with hexane to obtain desired compound (0.27 g, 89%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07977340B2 |
| Source dataset | uspto-grants-2011_07 |
| ORD ID | ord-18cbabfc64b647299b8469b8255a1d4b |
| Source note | uspto-grants-2011_07 |