HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl acetate hexane → HCID 67021312, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl acetate hexane | HCID 21226206 | — |
| Reactant | [4-(3-Amino-pyridin-2-ylamino)-2-chloro-phenyl]-acetic acid ethyl ester | HCID 67021554 | — |
| Product | HCID 67021312 | HCID 67021312 | — |
Reaction Steps
is obtained analogously to the method as described in Step 1.2 but using [4-(3-amino-pyridin-2-ylamino)-2-chloro-phenyl]-acetic acid ethyl ester instead of [4-(3-amino-pyridin-2-ylamino)-phenyl]-acetic acid methyl ester as a starting material. ES-MS: 316.1 [M+H]+; single peak at tR=4.24 min (System 1); Rf=0.16 (Hexane/EtOAc, 1:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07977338B2 |
| Source dataset | uspto-grants-2011_07 |
| ORD ID | ord-b7a335c219ca49a79174d277c441552f |
| Source note | uspto-grants-2011_07 |