Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 178478323 | HCID 178478323 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 178509092 | HCID 178509092 | — |
Reaction Steps
A mixture of 2,6-dichloro-1H-purine (5 g) and ammonia solution (79.2 mL, 2M in (isopropanol) was stirred and heated at 120° C. in an autoclave overnight. The reaction was cooled and concentrated in vacuo to give the title compound as an off-white solid in quantitative yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07977344B2 |
|---|
| Source dataset | uspto-grants-2011_07 |
|---|
| ORD ID | ord-0dc9f4da72324df487aaf546fdb439b4 |
|---|
| Source note | uspto-grants-2011_07 |
|---|
