Hydrochloric Acid → 74975-02-3

Participants

Reaction Conditions

Reaction Steps

To a stirred solution of 2,2-dimethyl-4-[(E)-2-(methyloxy)ethenyl]tetrahydro-2H-pyran (2.93 g, 17.21 mmol) in THF (15 ml) was added 2N HCl (15 ml, 30.0 mmol) and the mixture was stirred at 20° C. After 1 hour the mixture was extracted with diethyl ether (3×25 ml); the combined ether extracts dried (Na2SO4), filtered and evaporated in vacuo (at 50 mbar and water bath at 15° C.) to give the title compound as a pale yellow oil (2.56 g).

Provenance & Evidence