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HRID1011142

反应详情

EQUATION

反应方程式

HRID 1011142 的结构方程式

REACTANTS

反应物

2
结构：BrCCC1CCOCC1
HCID22637012

4-(2-Bromoethyl)oxane

C7H13BrO

结构：CCC[C@@H](C)Oc1nc2nc(OC)nc-2c(N)[nH]1.O=C(O)C(F)(F)F
HCID178448284

未命名化合物

PRODUCTS

生成物

1
结构：CCC[C@@H](C)Oc1nc(N)c2nc(OC)n(CCC3CCOCC3)c2n1
HCID57699789

未命名化合物

PROCEDURE

实验过程

Prepared similarly to Intermediate 223 from 2-{[(1R)-1-methylbutyl]oxy}-8-(methyloxy)-1H-purin-6-amine trifluoroacetate and 4-(2-bromoethyl)tetrahydro-2H-pyran but conducting the alkylation over 1 hour at 60° C.

WORKUP

后处理

  1. customover 1 hour
  2. customat 60° C.