HRID1011151

反应详情

EQUATION

反应方程式

HRID 1011151 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

To a solution of N2-butyl-8-methoxy-9-(tetrahydro-2H-pyran-2-ylmethyl)-9H-purine-2,6-diamine in dry methanol (5 ml) at room temperature and under nitrogen was added 4.0M hydrogen chloride in 1,4-dioxane (1.5 ml) in one go. The reaction was left to stir at room temperature overnight. The reaction was concentrated in vacuo and the product purified by MDAP. This afforded the title compound 6 mg (slower-running on MDAP).

WORKUP

后处理

  1. waitThe reaction was left
  2. concentrationThe reaction was concentrated in vacuo
  3. customthe product purified by MDAP