HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron trifluoride → HCID 87318249, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron trifluoride | HCID 6356 | — |
| Reactant | HCID 67234273 | HCID 67234273 | — |
| Product | HCID 87318249 | HCID 87318249 | — |
Reaction Steps
From 1.0 g of 8,9-difluoro-3-methyl-7-oxo-2,3-dihydro-7H-[1,4]oxazino[2,3,4-ij]quinoline-6-carboxylic acid (for preparation see Journal of Medicinal Chemistry 1992, 35 (4), 611) and 1.51 g (3 eq.) of BF3 etherate, by the same method as described for Example 38A, 1.0 g (85% of theory) of the title compound is isolated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07977349B2 |
| Source dataset | uspto-grants-2011_07 |
| ORD ID | ord-02c1b1ccdc124bb5bc508dc6b8bbead1 |
| Source note | uspto-grants-2011_07 |