HRID1011254

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：C[C@@H]1CN(c2ccc([N+](=O)[O-])cc2F)[C@@H](C)CN1C

HCID57664351

未命名化合物

结构：C[C@@H]1CN(c2ccc([N+](=O)[O-])cc2F)C[C@H](C)N1

HCID57664386

未命名化合物

PRODUCTS

生成物

结构：C[C@@H]1CN(c2ccc([N+](=O)[O-])cc2F)C[C@H](C)N1C

HCID57664380

未命名化合物

收率 100%

PROCEDURE

实验过程

Crude cis-4-(2-Fluoro-4-nitrophenyl)-1,2,6-trimethylpiperazine (6.1 g, 100% recovery) is prepared according to the method described above for the synthesis of racemic-1-(2-fluoro-4-nitrophenyl)-trans-2,4,5-trimethylpiperazine from 1-(2-fluoro-4-nitrophenyl)-cis-3,5-dimethylpiperazine (5.71 g, 24.2 mmol). LCMS-ESI (m/z): calcd for C13HBFN3O2, 267; [M+H]+ found, 268.