1,2-Ethanediamine, N1,N1-diethyl-N2-methyl- → HCID 59665587, compound

HRID 1011344Notes

Reaction equation

HRID 1011344 reaction equation
[O:1]=[C:2]1[C:10]2[C:5](=[N:6][C:7]([CH:11]=O)=[CH:8][CH:9]=2)[CH2:4][O:3]1.[CH2:13]([N:15]([CH2:20][CH3:21])[CH2:16][CH2:17][NH:18][CH3:19])[CH3:14]>>[CH2:13]([N:15]([CH2:20][CH3:21])[CH2:16][CH2:17][N:18]([CH2:11][C:7]1[N:6]=[C:5]2[CH2:4][O:3][C:2](=[O:1])[C:10]2=[CH:9][CH:8]=1)[CH3:19])[CH3:14]

Participants

3

Reactant 2

HCID 660341,2-Ethanediamine, N1,N1-diethyl-N2-methyl-HCID 58478784HCID 58478784, compound

Product 1

HCID 59665587HCID 59665587, compoundYield 64%

Procedure

In a process similar to that described in Preparation 8, 5-oxo-5,7-dihydro-furo[3,4-b]pyridine-2-carbaldehyde (110 mg, 0.68 mmol) and N,N-diethyl-N′-methylethylenediamine (109 μL, 0.68 mmol) are reacted to provide the title compound as white solid (120 mg, 64%).

Workup

  1. customare reacted

Sources & evidence

ORD record
ord-cf7fdc1b943b4e2b9754377f17ddae09
Source dataset
uspto-grants-2011_07
Patent number
US07977351B2

Reaction notes

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