HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Ethanediamine, N1,N1-diethyl-N2-methyl- → HCID 59665587, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Ethanediamine, N1,N1-diethyl-N2-methyl- | HCID 66034 | — |
| Reactant | HCID 58478784 | HCID 58478784 | — |
| Product | HCID 59665587 | HCID 59665587 | 64% |
Reaction Steps
In a process similar to that described in Preparation 8, 5-oxo-5,7-dihydro-furo[3,4-b]pyridine-2-carbaldehyde (110 mg, 0.68 mmol) and N,N-diethyl-N′-methylethylenediamine (109 μL, 0.68 mmol) are reacted to provide the title compound as white solid (120 mg, 64%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07977351B2 |
| Source dataset | uspto-grants-2011_07 |
| ORD ID | ord-cf7fdc1b943b4e2b9754377f17ddae09 |
| Source note | uspto-grants-2011_07 |