1,2-Ethanediamine, N1,N1-diethyl-N2-methyl- → HCID 58478793, compound

HRID 1011381Notes

Reaction equation

HRID 1011381 reaction equation
[O:1]=[C:2]1[C:10]2[C:5](=[N:6][C:7]([CH2:11][CH2:12][CH:13]=O)=[CH:8][CH:9]=2)[CH2:4][O:3]1.[CH2:15]([N:17]([CH2:22][CH3:23])[CH2:18][CH2:19][NH:20][CH3:21])[CH3:16]>>[CH2:15]([N:17]([CH2:22][CH3:23])[CH2:18][CH2:19][N:20]([CH3:21])[CH2:13][CH2:12][CH2:11][C:7]1[N:6]=[C:5]2[CH2:4][O:3][C:2](=[O:1])[C:10]2=[CH:9][CH:8]=1)[CH3:16]

Participants

3

Reactant 2

HCID 660341,2-Ethanediamine, N1,N1-diethyl-N2-methyl-HCID 58478730HCID 58478730, compound

Product 1

HCID 58478793HCID 58478793, compoundYield 65.5%

Procedure

In a process similar to that described in Preparation 8, 3-(5-Oxo-5,7-dihydro-furo[3,4-b]pyridin-2-yl)-propionaldehyde (63 mg, 0.33 mmol) and N,N-diethyl-N′-methylethylenediamine (43 mg, 0.32 mmol) are reacted to provide the title compound as white solid (64 mg, 63%).

Workup

  1. customare reacted

Sources & evidence

ORD record
ord-e19d4462d3aa4f5b980bf241f7f01949
Source dataset
uspto-grants-2011_07
Patent number
US07977351B2

Reaction notes

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