HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Ethanediamine, N1,N1-diethyl-N2-methyl- → HCID 58478793, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Ethanediamine, N1,N1-diethyl-N2-methyl- | HCID 66034 | — |
| Reactant | HCID 58478730 | HCID 58478730 | — |
| Product | HCID 58478793 | HCID 58478793 | 65.5% |
Reaction Steps
In a process similar to that described in Preparation 8, 3-(5-Oxo-5,7-dihydro-furo[3,4-b]pyridin-2-yl)-propionaldehyde (63 mg, 0.33 mmol) and N,N-diethyl-N′-methylethylenediamine (43 mg, 0.32 mmol) are reacted to provide the title compound as white solid (64 mg, 63%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07977351B2 |
| Source dataset | uspto-grants-2011_07 |
| ORD ID | ord-e19d4462d3aa4f5b980bf241f7f01949 |
| Source note | uspto-grants-2011_07 |