HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium Hydroxide → HCID 23159767, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium Hydroxide | HCID 3939 | — |
| Reactant | HCID 23159744 | HCID 23159744 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 23159767 | HCID 23159767 | — |
Reaction Steps
A solution of ethyl 5-benzyloxyquinoline-3-carboxylate (3.07 g, 10 mmol) prepared in stage A and LiOH (0.4 g, 20 mmol) in THF (20 mL)and water (0.5 mL) was refluxed for 2 hours. After cooling, the solvents were evaporated under vacuum. The solid residue was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07977354B2 |
| Source dataset | uspto-grants-2011_07 |
| ORD ID | ord-2fe2595dad2c42a7a6f6bc0ac23bf8f9 |
| Source note | uspto-grants-2011_07 |