Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Trifluoroacetic anhydride | HCID 9845 | — |
| Reactant | HCID 23159787 | HCID 23159787 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 23159782 | HCID 23159782 | — |
Reaction Steps
To a solution of 3-(methylsulfinyl)-5-methoxyquinoline (2.21 g, 10 mmol) in CH2Cl2 (50 mL) is added TFAA. The resulting solution is stirred at 20-50° C. for 1 hour. The solution is then treated with NEt3 affording the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07977354B2 |
|---|
| Source dataset | uspto-grants-2011_07 |
|---|
| ORD ID | ord-fcc3396e5bc64003a33717bb5420ebf3 |
|---|
| Source note | uspto-grants-2011_07 |
|---|
