HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Methoxide → HCID 14837017, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | 3-Bromo-5-(trifluoromethyl)pyridine | HCID 11127991 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 14837017 | HCID 14837017 | — |
Reaction Steps
To a solution of 3-bromo-5-trifluoromethylpyridin (2.25 g 10 mmol, prepared as described in Eur. J. Org. Chem. 2002, 327-330, in DMF was added sodium methoxide (0.8 g, 15 mmol). The resultant solution is stirred for 20 hours at 40° C. The title compound is obtained after evaporation of the solvent under vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07977354B2 |
| Source dataset | uspto-grants-2011_07 |
| ORD ID | ord-e6acd3dd604048d7943ed3a728da25f3 |
| Source note | uspto-grants-2011_07 |